RF Conductivity Measurement of Conductive Zell Fabric
 Author: Nguyen Tien Manh, Chung JaeYoung
 Publish: Journal of electromagnetic engineering and science Volume 16, Issue1, p24~28, 31 Jan 2016

ABSTRACT
This study presents a conductivity measurement technique that is applicable at radio frequencies (RF). Of particular interest is the measurement of the RF conductivity of a flexible Zell fabric, which is often used to implement wearable antennas on clothes. First, the transmission coefficient is measured using a planar microstrip ring resonator, where the ring is made of a Zell fabric. Then, the fabric’s conductivity is determined by comparing the measured transmission coefficient to a set of simulation data. Specifically, a MATLAB based rootsearching algorithm is used to find the minimum of an error function composed of measured and simulation data. Several error functions have been tested, and the results showed that an error function employing only the magnitude of the transmission coefficient was the best for determining the conductivity. The effectiveness of this technique is verified by the measurement of a known copper foil before characterizing the Zell fabric. The conductivity of the Zell fabric at 2 GHz appears to be within the order of 10^{4} S/m, which is lower than the DC conductivity of 5×10^{5} S/m.

KEYWORD
Conductivity , Material Characterization , Ring Resonator , Zell Fabric

I. INTRODUCTION
In recent years, wearable antennas for bodyworn communication systems have been studied extensively [1]. One way to realize such antennas is by using conductive fabrics [2]. Such fabrics are highly flexible, durable, and restorable, and they can be directly integrated onto clothing by ordinary sewing or embroidering techniques. To derive an appropriate antenna design, it is essential to have accurate information about the electrical properties of conductive fabrics, especially the conductivity (
σ ) at the antenna’s operation frequency.Commonly, the manufacturers of conductive fabrics provide the DC sheet resistances (
R_{s} ) measured by the wellknown fourpoint probe or van der Pauw methods [3,4]. The DC sheet resistance values range from 0.02 to 0.8 Ω/sq [5], implying that the DC conductivity ranges froms =1.2×10^{4} to 5×10^{5} S/m based on the formulas =1/(R_{s} ×t ), wheret is the thickness of the fabric. This study aims to measure the RF conductivity instead of the DC one to realize accurate modeling of wearable antennas.Many studies have measured the RF permittivity of dielectrics. However, few studies have measured the conductivity of highly conductive materials at RF. In [6,7], a planar resonator is used as a test fixture to measure the quality factor (Qfactor) with the conductor under test inserted in. Then, the conductor’s
σ is obtained from a closedform equation of the Qfactor under the assumption that the dielectric and radiation losses are trivial. However, in practice, these losses may distort the resultingσ , and they should not be underestimated.As an alternative, fullwave simulation data can be used to estimate the conductivity instead of the approximate closedform equations.In a fullwave simulation tool, a structure identical to the material under test is modeled, and then, the simulation data is collected by varying the material properties (e.g.,
σ ). Subsequently, the measured and simulated data are compared in a rootsearching algorithm to find the best fit. Recent reports have verified the effectiveness of this method for the measurement of the dielectric constant (ε_{r} ) and loss tangent (tanδ ) of an antenna substrate [8,9].In this paper, we present a conductivity measurement method by employing a planar ring resonator (shown in Fig. 1) and surrogatebased optimization (SBO) [10] as the rootsearching tool. Section II provides an outline of the measurement process. Section III demonstrates the effectiveness of the proposed method by measuring a copper ring with known conductivity. Section IV discusses the conductivity measurement of the Zell fabric. The results appear to be within the order of 10^{4} S/m, which is lower than the DC conductivity of the order of 10^{5} S/m reported by the manufacturer.
II. OVERVIEW OF PROPOSED MEASUREMENT METHOD
Fig. 2 shows a flowchart of the conductivity measurement process. A microstrip ring resonator with
H =1.6 mm,W =90 mm, andL =140.3 mm is fabricated on a FR4 substrate to measure the transmission coefficient (S _{21}). This resonator is fabricated to exhibit a resonance of around 2 GHz, which is the frequency of interest. The transmission lines between the ports and ring are made of copper, and the ring is made of the material under test. The main radius of the ring isR =25.9 mm, and the width of both the ring and the transmission lines isw_{l} =3.2 mm to conform to the 50Ω impedance matching condition at 2 GHz. The coupling gap separating the feeding lines from the ring should have an appropriate size to avoid any effect on the fields of the resonant structure and to minimize losses. Specifically, the gap is set to 0.64 mm to support resonance around 2 GHz based on the ring resonator design equation found elsewhere [11].Meanwhile, a resonator identical to the fabricated one is modeled in a fullwave simulation tool (Ansys HFSS). The conductivity of the ring in the simulation model is varied to collect a set of
S _{21} data, as shown in the righthandside branch in Fig. 2. The measuredS _{21} and the set of simulatedS _{21} values are then compared in an error function formulated using the magnitude and phase ofS _{21}. The conductivity of the unknown fabric is determined when the error function becomes zero (or close to zero). We use SBO as the iterative comparator to efficiently search for aσ value that minimizes the error function. SBO is widely used to find solutions of nonlinear electromagnetic problems as it offers an efficient iterative scheme by intelligently choosing the best sampling and evaluation strategies. In this work, the MATLAB toolbox for SBO providedby Ghent University, Belgium [12] is used.III. MEASUREMENT WITH COPPER RING RESONATOR
The proposed measurement method is first tested with a ring made of copper. Fig. 3 shows the fabricated copper ring resonator and Fig. 4, the measured and simulated
S _{21} magnitudes. For the simulation data,S _{21} is collected by varyings of the ring from 10^{7} to 10^{8} S/m with an interval of 10^{0.0625} (i.e., 17 points are considered). As can be observed, the resonator is correctly designed to resonate around 2 GHz, and only a slight perturbation is observed in the simulation results as the copper conductivity is high enough.The set of simulated
S _{21} values is compared with the measuredS _{21} value using an error function in the SBO process. The error function should be formulated carefully to obtain an accurate result. Initially, we used an error function composed of only the magnitude ofS _{21}, namely,where are the magnitudes of the simulation and measurement at the resonant frequency. Fig. 5 shows the error function values along the sampled conductivity points and the interpolated Kriging model after the SBO process. The error function is minimum at
σ =10^{7.24} (1.74×10^{7} S/m). This retrieved conductivity is lower than the DC conductivity of pure bulk copper (σ =5.7×10^{7} S/m) and is close to the conductivity of plated copper at microwave frequency [13,14]. It is also known that the conductivity becomes lower as the frequency increases owing to the skin effect and surface roughness.IV. MEASUREMENT OF ZELL FABRIC
After measuring the conductivity of copper using the proposed method, we measured the conductivity of the Zell fabric, a metalized nylon fabric. The Zell fabric under test has a thickness of 0.1 mm and DC surface resistance as low as 0.02 Ω/sq [5], corresponding to a DC conductivity of 5×10^{5} S/m.
Fig. 6 shows the microstrip ring resonator with the ring made of Zell fabric. The Zell fabric ring is attached on the FR4 substrate using fastdrying urethane glue. The glue has trivial influence on the resonator performance because its layer is very thin and its relative permittivity (3.2 at 23℃) is close to that of the FR4 used. On the other hand, a ring resonator with the same dimension as that shown in Fig. 6 was modeled in the fullwave EM simulator, and
S _{21} values were obtained by varying the conductivity of the ring from 10^{3.75} to 10^{6} S/m. pecifically, 37 values were collected with an interval of 10^{0.0625} S/m. Fig. 7 shows the measured and simulatedS _{21} magnitude data. The measurement is performed using Anritsu Vector Network Analyzer MS2038C, which as measurement uncertainty of 0.04 dB around 2 GHz.As shown in Fig. 7, the simulated
S _{21} peak is broader and lower for the ring with lower conductivity, and the measured data falls somewhere within the simulated conductivity range.For the conductivity retrieval process, we test four different error functions in addition to
EF _{1} in the previous section. The other three arewhere are the phase of the simulated and measured
S _{21} at the resonant frequency, respectively. InEF _{3} andEF _{4}, the arithmetic mean ofS _{21} is used by averagingS _{21} data over a 300MHz bandwidth (i.e., 31 frequency points). Here,h andl are index numbers of the frequencies that are 150 MHz higher and lower than the resonant frequency, respectively. The constantsa andb inEF _{2} andEF _{4} are scaling factors to compensate for the difference of order between the magnitude and phase, respectively.The SBO toolbox compares the simulated and measured data using the abovementioned error functions to determine the conductivity of the Zell fabric. Fig. 8(a)–(d) show the resulting Kriging models when
EF _{1} toEF _{4} are considered, respectively.The error function minima for
EF _{1},EF _{2},EF _{3}, andEF _{4} are located atσ =10^{4.335} (2.16×10^{4} S/m), 10^{4.38} (2.4×10^{4} S/m), 10^{4.11} (1.29×10^{4} S/m), and 10^{4.11} (1.29×10^{4} S/m), respectively. The consistency among these error functions demonstrates that including the phase (e.g.,EF _{2}) or averaging over a bandwidth (e.g.,EF _{3} andEF _{4}) does not alter the obtained conductivity value. This implies that formulating the error function using only theS _{21} magnitude (e.g.,EF _{3}) is sufficient to evaluate the conductivity using the proposed method. Furthermore, it should be noted that the measured conductivity of the Zell fabric at 2 GHz shows an order difference from the DC conductivity given by the manufacturer (5×10^{5} S/m) [5]. This may be due to the significant ohmic loss as well as the surface roughness seen at the microwave frequency.V. CONCLUSION
In this paper, a new measurement technique for evaluating RF conductivity is described. The proposed method employs a microstrip ring resonator, fullwave simulation data, and SBO optimization technique to measure the conductivity of a conductive fabric at a microwave frequency. We first evaluated the conductivity of plated copper using the proposed method, and then, we applied it to measure the conductivity of a Zell fabric. For both cases, the conductivity values around 2 GHz were lower than the known DC conductivity. This is because highfrequency currents mostly flow along the surface owing to the skin effect and concurrent influence of the surface roughness of the conductor. Therefore, it is important to measure the highfrequency conductivity of newly introduced conductive materials to formulate an accurate model of antennas and RF components.

5.

[Fig. 1.] Geometry of microstrip ring resonators. The ring is made of the material under test.

[Fig. 2.] Flow chart of the conductivity measurement process.

[Fig. 3.] Fabricated copper ring resonator

[Fig. 4.] Simulated and measured S21 of copper ring resonator (simulation from σ=107 to 108 S/m).

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[Fig. 5.] Error function values and corresponding Kriging model from surrogatebased optimization (SBO) process.

[Fig. 6.] Fabricated Zell ring resonator.

[Fig. 7.] Simulated and measured S21 values of Zell ring resonator.

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[Fig. 8.] (a？d) Error function values and corresponding Kriging models from surrogatebased optimization (SBO) process.